[{"ID":"1557","Title":"通微 2020 版新药典解决方案: HPLC-ELSD 检测酸枣仁中酸枣仁皂苷 A","Describe":"酸枣仁为鼠李科植物酸枣的干燥成熟种子，具有养心安神的功效，是较为常用的镇静催眠中药。酸枣仁皂苷 A 为其镇静催眠的有效成分之一。酸枣仁皂苷 A 的含量测定可以有效监测酸枣仁质量。酸枣仁皂苷 A 为三萜皂苷类成分，紫外吸收弱，不宜采用 UV 检测，而采用质量型通用型检测器 ELSD 则可有效避免上述问题，实现酸枣仁中酸枣仁皂苷 A 的含量测定。","CompanyName":"上海通微分析技术有限公司","PgID":"171","CompanyID":"369111","CreateTime":"2021-04-09","HitNumber":"193","Name":"药材和饮片","ClassID":"21985","ClassName":"制药","FClassID":"21640","FilePath":"2/20210409/637535781145161139833.pdf","FileDomain":"img77","IsDownload":"1","SecondData":[{"ID":"2575","ProductID":"34340581","Type":"EasySep®3030","Name":"EasySep®3030 HPLC高效液相色谱","PictureDomain":"img68","Picture":"2/20200513/637250097354590076756.jpg","IsZhuTui":"1","UserID":"371443"}]},{"ID":"1430","Title":"金银花中多种禁用农药及相关化学品残留的测定解决方案","Describe":"本文参照2020版《中国药典》2341通则农药残留量测定法新增第五法《药材及饮片（植物类）中禁用农药多残留测定法》中的固相萃取法，使用乙腈对金银花试样进行均质提取，经盐析和离心后，GC-MS/MS组化合物采用GCB/NH2柱净化，LC-MS/MS组化合物采用HLB柱净化，后上机检测。","CompanyName":"睿科集团股份有限公司","PgID":"183","CompanyID":"263077","CreateTime":"2021-02-25","HitNumber":"108","Name":"药材和饮片","ClassID":"21985","ClassName":"制药","FClassID":"21640","FilePath":"2/20210225/637498668511910456510.pdf","FileDomain":"img77","IsDownload":"1","SecondData":[{"ID":"2377","ProductID":"34846202","Type":"","Name":"睿科 AH-50全自动均质器","PictureDomain":"img80","Picture":"2/20210107/637456283924685164760.png","IsZhuTui":"1","UserID":"254446"}]},{"ID":"1415","Title":"枸杞子中甜菜碱的检测","Describe":"本方案适用于枸杞中甜菜碱的检测。枸杞子：本品为茄科植物宁夏枸杞Lycium barbarum L.的干燥成熟果实。夏、秋二季果实呈红色时采收，热风烘干，除去果梗，或晾至皮皱后，晒干，除去果梗。2020 版《中国药典》一部 枸杞子【含量测定】项下甜菜碱的测定，将之前的薄层色谱法改为高效液相色谱法，前处理采用碱性氧化铝固相萃取柱净化。","CompanyName":"北京迪科马科技有限公司（迪马科技）","PgID":"174","CompanyID":"150167","CreateTime":"2021-02-05","HitNumber":"301","Name":"药材和饮片","ClassID":"21985","ClassName":"制药","FClassID":"21640","FilePath":"2/20210205/637481405361554173855.docx","FileDomain":"img76","IsDownload":"0","SecondData":[{"ID":"2310","ProductID":"24754160","Type":"","Name":"低温蒸发光散射检测器","PictureDomain":"img68","Picture":"2/20200107/637140108262093459705.jpg","IsZhuTui":"1","UserID":"133732"}]},{"ID":"1397","Title":"基于仿生技术的制川乌炮制过程变化研究","Describe":"本实验将电子鼻、电子舌仿生技术运用于制川乌炮制过程“气”“味”变化研究，将传统的“气”“味”信息进行了数字量化表征，并与制川乌炮制过程中内在有效成分变化进行了相关性分析，为中药炮制研究提供了一-种新的思路。","CompanyName":"北京盈盛恒泰科技有限责任公司","PgID":"171","CompanyID":"7254","CreateTime":"2021-01-28","HitNumber":"510","Name":"药材和饮片","ClassID":"21985","ClassName":"制药","FClassID":"21640","FilePath":"2/20210128/637474495328122777818.pdf","FileDomain":"img76","IsDownload":"0","SecondData":[{"ID":"2287","ProductID":"6033903","Type":"TS-5000Z","Name":"日本INSENT味觉分析系统（电子舌）","PictureDomain":"img46","Picture":"2/20110830/634503074867507500.jpg","IsZhuTui":"1","UserID":"23068"}]},{"ID":"1371","Title":"高效液相色谱测定小蓟中芦丁含量","Describe":"小蓟为菊科植物小蓟的干燥地上部分或根、具有凉血止血、祛瘀消肿的功能，可用于治疗衄血、吐血、尿血、便血、崩漏、外伤出血、痈肿疮毒等。小蓟中所含有机酸中有芦丁、咖啡酸等，文献记载芦丁、咖啡酸为其止血活性成分。本实验采用高效液相色谱法测定小蓟中芦丁的含量，方法稳定、快速、重现性好。","CompanyName":"南京科捷分析仪器有限公司","PgID":"174","CompanyID":"527","CreateTime":"2021-01-15","HitNumber":"151","Name":"药材和饮片","ClassID":"21985","ClassName":"制药","FClassID":"21640","FilePath":"2/20210115/637463223405705891442.pdf","FileDomain":"img77","IsDownload":"0","SecondData":[{"ID":"2255","ProductID":"29729691","Type":"LC-600A","Name":"高效液相色谱仪","PictureDomain":"img78","Picture":"2/20201120/637414626569098951755.jpg","IsZhuTui":"1","UserID":"190"}]},{"ID":"1168","Title":"利用三重四极杆GC-MS/MS系统采用快速溶剂萃取完成草药中的多农残分析","Describe":"本应用报告说明了利用快速溶剂萃取（ASE）和凝胶渗透色谱法（GPC）进行草药产品中多农残分析的方法。所采用检测和定量系统为TSQ 8000 GC-MS/MS。 将200多种农残化合物的日常筛选方法应用到一系列不同 样品类型上，从普通 红茶或者鼠尾草，以及茴香种子和医学用途的药草，到香料用途的百里香和甘菊。采用Thermo Scientific TraceFinder定量软件包进行数据处理和报告。","CompanyName":"赛默飞色谱及质谱","PgID":"171","CompanyID":"915","CreateTime":"2020-10-23","HitNumber":"413","Name":"药材和饮片","ClassID":"21985","ClassName":"制药","FClassID":"21640","FilePath":"2/20201023/637390416901540908553.pdf","FileDomain":"img73","IsDownload":"0","SecondData":[{"ID":"1991","ProductID":"25159172","Type":"TSQ 8000 Evo","Name":"赛默飞三重四极杆气质联用仪","PictureDomain":"img47","Picture":"2/20181221/636810018565039396992.jpg","IsZhuTui":"1","UserID":"785"}]},{"ID":"935","Title":"ICP-MS 2000E测定黄芪中铜、砷、镉、汞、铅五种重金属元素","Describe":"本文参考中华人民共和国药典（2015）版四部通则（2321）铜、砷、镉、汞、铅测定法，使用ICP-MS 2000E电感耦合等离子体质谱仪，测定GBW10028（GSB-19）黄芪中五种重金属元素含量。","CompanyName":"江苏天瑞仪器股份有限公司","PgID":"174","CompanyID":"18507","CreateTime":"2020-08-05","HitNumber":"236","Name":"药材和饮片","ClassID":"21985","ClassName":"制药","FClassID":"21640","FilePath":"2/20200805/637322227896113412144.doc","FileDomain":"img75","IsDownload":"0","SecondData":[{"ID":"1690","ProductID":"7653557","Type":"ICP-MS 2000系列","Name":"电感耦合等离子体质谱仪","PictureDomain":"img70","Picture":"2/20191115/637094126787034683541.jpg","IsZhuTui":"1","UserID":"49221"}]},{"ID":"905","Title":"原子吸收分光光度计检验药品中金属元素方法","Describe":"依据2020版中国药典使用上海光谱3803AA原子吸收光谱仪检测中药药材及饮品中重金属元素。","CompanyName":"上海光谱仪器有限公司","PgID":"174","CompanyID":"333069","CreateTime":"2020-07-22","HitNumber":"966","Name":"药材和饮片","ClassID":"21985","ClassName":"制药","FClassID":"21640","FilePath":"2/20200722/637310332403744990247.pdf","FileDomain":"img73","IsDownload":"1","SecondData":[{"ID":"1643","ProductID":"24929836","Type":"SP-3803AA","Name":"双光束原子吸收分光光度计","PictureDomain":"img53","Picture":"2/20160704/636032419846362279724.jpg","IsZhuTui":"1","UserID":"332448"}]},{"ID":"843","Title":"参照2015年版《中国药典》测定甘草苷含量","Describe":"采用TSKgel ODS-100V色谱柱，参考2015年中国药典方法分析甘草苷，甘草苷和甘草酸分离良好，柱效可满足药典规定大于5000的要求。","CompanyName":"东曹（上海）生物科技有限公司","PgID":"174","CompanyID":"236165","CreateTime":"2020-07-01","HitNumber":"1850","Name":"药材和饮片","ClassID":"21985","ClassName":"制药","FClassID":"21640","FilePath":"2/20200701/637292363205790872416.pdf","FileDomain":"img75","IsDownload":"1","SecondData":[{"ID":"1554","ProductID":"23658109","Type":"TSKgel ODS-100V","Name":"C18反相色谱柱","PictureDomain":"img66","Picture":"2/20160111/635881168202989944124.jpg","IsZhuTui":"1","UserID":"223469"}]},{"ID":"545","Title":"柴胡注射液中正己醛的测定应用方案","Describe":"本方法参考药典中柴胡注射液，采用顶空-气相色谱检测，测定柴胡注射液中正己醛的含量。","CompanyName":"上海舜宇恒平科学仪器有限公司","PgID":"174","CompanyID":"9751","CreateTime":"2020-03-09","HitNumber":"348","Name":"药材和饮片","ClassID":"21985","ClassName":"制药","FClassID":"21640","FilePath":"2/20200309/637193478938041234186.pdf","FileDomain":"img71","IsDownload":"0","SecondData":[{"ID":"1004","ProductID":"29840779","Type":"GC1290","Name":"国产气相色谱","PictureDomain":"img69","Picture":"2/20190418/636911993188201086583.jpg","IsZhuTui":"1","UserID":"34124"},{"ID":"1003","ProductID":"157204","Type":"","Name":"FA电子分析天平","PictureDomain":"img71","Picture":"2/20190408/636903156564402796711.jpg","IsZhuTui":"0","UserID":"34124"}]}]